Accelerated solvent extraction coupled to GC-MS/MS for the analysis of atractylenolide in Atractylodes macrocephala
文献类型： 外文期刊
作者： Liao, Qie Gen 1 ; Li, Rui Li 1 ; Luo, Lin Guang 1 ;
作者机构： 1.Jiangxi Acad Agr Sci, Jiangxi Acad Agr Sci Key Lab Qual & Safety Agr Pr, Agr Prod Qual Safety & Stand Inst, Nanchang 330200, Peoples R China
关键词： Accelerated solvent extraction (ASE);Atractylenolide (AO);Atractylodes macrocephala;Gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS)
期刊名称：CHROMATOGRAPHIA （ 影响因子：2.044； 五年影响因子：1.725 ）
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收录情况： SCI
摘要： The performance of accelerated solvent extraction (ASE) in the analysis of atractylenolide I (AO-I) and atractylenolide III (AO-III) in Atractylodes macrocephala rhizome samples was investigated and compared with that of Soxhlet extraction (SE) and ultrasonically assisted extraction in terms of yield, extraction time, reproducibility, and solvent consumption. The results indicated that although the highest yield was achieved by SE, ASE appears to be a promising alternative to classical methods because it is faster and requires less solvent, especially when investigating large batches of plant samples. The use of ethanol at a temperature of 100 °C, performing two extraction cycles with a static duration of 10.0 min, represented the optimal ASE parameters. The extracts were analyzed by gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS).
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